Micromeritics instrument corporation chemical technology. Microactive for autopore v provides the ability to overlay up to 20 runs. Autopore iv 9500 is a shareware software in the category miscellaneous developed by autopore iv 9500. Autopore iv 9500 runs on the following operating systems. We can remember when we had to manually fill the penetrometers and increase the pressure by means of a dial.
Included is the option to import pore size distributions from gas adsorption isotherms to provide analysis data in the micro to macropore range in a single report overlay multiple runs and gas adsorption data pore volume, pore area, and pore size plots are available as. Because we have found no equal in the marketplace for reliability, repeatability, and ease of use. These include pore size distributions, total pore volume, total pore surface area, median pore diameter and sample densities bulk and skeletal. Micromeritics autopore iv research facilities chemical. The autopore features several levels of mechanical and electromechanical safety devices. Micromeritics autopore iv 9510 characterizes a material porosity by applying various levels of pressure to a sample immersed in mercury. Autopore v automated mercury porosimeter from micromeritics. Micromeritics products brochure micromeritics instrument. Micromeritics tristar ii plus surface area analyzer. This instrument also features enhanced safety features and offers new data reduction and reporting choices that provide more information about pore geometry and the fluid transport characteristics of your material. Our latest offering, the autopore iv series of mercury porosimeters, provides the same highquality analysis data as expected from other micromeritics products and, in addition, comes with enhanced data reduction and. Particle and surface sciences is supplying the autopore iv 9500 series from micromeritics.
Paper open access workability and mechanical property of. The autopore iv software allows you to enter the precise angle of contact between mercury and a solid sample surface. Autopore iv 9500 has not been rated by our users yet. Static volumetric chemisorption analysis sample report.
Technique the geopyc automatically determines the volume and density of a solid object by displacement of dry flo, a solid medium. Micromeritics if, at the request of the purchaser, micromeritics modifies a standard product or manufactures a special product to the purchasers specifications. Porosity and its influence on pharmaceutical tablet. Check pages 1 6 of autopore iv series micromeritics in the flip pdf version. Syllabus autopore series advanced operator training click here to download full course details instructional goals. Mercury intrusion porosimeter scientific and technical. At different time points of 2, 6, 10, 24, 48, and 72 h the samples. Flowsorb iii 2305 2310 micromeritics instrument corp. Model 9505 from atmospheric pressure to 33,000 psia 228 mpa model 9520 from atmospheric pressure to 60,000 psia 414 mpa pore diameter. The medium is a narrow distribution of small, rigid spheres that have a high degree of flow ability and achieve close packing around the object under investigation. You can enter values for the advancing contact angle intrusion, receding contact angle extrusion, and mercury surface tension. Click here to download the autopore iv series porosimeters brochure in pdf. This document will provide a detailed operation procedure of the micromeritics autopore iv po rosimeter.
Mercury intrusion pressure is raised automatically, up to 220 mpa, and intruded volume into sample is related with porosity determination. Micromeritics autopore iv 9500 series characterizes a materials porosity by applying various levels of pressure to a sample immersed in mercury. Have regular exposure to an autopore in a laboratory. This course introduces students to advanced mercury porosimetry theory, applications, and data interpretation. Syllabus autopore 95xx operator training click here to download full course details instructional goals.
Autopore iv 95xx basic operator training learning center. The autopore iv 9605 series has 4 lowpressure ports and 2 highpressure ports for analys. Micromeritics autopore iv 9500 particle technology labs. With handson and classroom training, these courses are essential for laboratory personnel who require indepth knowledge of their instrument operation and its associated. This course introduces students to the components, operation, and theory of the autopore for mercury porosimetry. Mineralogy and permeability of gas and oil dolomite. Particle and surface sciences distributes autopore iv 9500. Micromeritics autopore v series offers the following advantages. We have been using micromeritics autopore technology since its early beginnings. Mar 24, 2010 the autopore iv 9500 series of mercury porosimeters from micromeritics enable the user to calculate numerous sample properties.
The autopore iv 9500 series is designed to test the porosity of materials by applying various levels of. To request a quote or additional product information, visit micromeritics web site at. Mercury intrusion porosimetry mip is a powerful technique utilized for the evaluation of porosity, pore size. Be able to identify and power up the system, including installation of the operating program.
Dynamic or pulse chemisorption analysis sample report. Synthesis of a green nanosilica material using beneficiated waste dunites. Autopore iv series autopore iv series mercury porosimeter 9500 and 9510 micromeritics autopore iv 9500 series characterizes a materials porosity by applying various levels of pressure to a sample immersed in mercury. The autopore v series mercury porosimeters can determine a broader pore size distribution more quickly and accurately than other methods. This instrument also features enhanced safety features and offers new data reduction and reporting choices that provide more information about pore geometry and the fluid transport characteristics of your. Micromeritics autopore iv 9500 series characterizes a materials porosity by. Having knowledge of the true andor apparent density of a material feedstock is important to the powder bed formation and sintering kinetics as well as the porosity, or indeed lack of porosity in the final product. Micromeritics training center micromeritics offers basic and advanced training for many of our instruments and applications in the norcross atlanta, georgia training center. The autopore v series mercury porosimeters can determine a broader pore size distribution more quickly and accurately. Autopore iv advantages ability to measure pore diameters from 0. Mercury intrusion porosimetry mip is a powerful technique utilized for the evaluation of porosity, pore size distribution, and pore volume among others to characterize a wide variety of solid and powder materials. Surface area true density is an inherent property of a material, whilst apparent density takes account of occluded voids within a material. Micromeritics instrument corporation autopore iv 9500 v1. Mercury porosimetry is a fast and precise technique for porosity characterization with a broad measurement range, suitable for a wide range of sample types.
Other collected fragments were were used for sem tests. Micromeritics autopore iv 9500 series 9505 automated. Micromeritics autopore iv 9510 characterizes a material porosity by applying various levels of. The equipment works within the pressure range from almost zero up to 414 mpa, which makes it possible to. Micromeritics autopore iv mercury intrusion porosimetry up to 60,000 psi for measurement of meso and macro pore size distribution, as well as solid density, particle density, skeletal density. Porosity and its influence on pharmaceutical tablet dissolution. Porosity was evaluated by using the settime equilibrium 10 s mode between the pressure limits of 0. Total plastics waste treatments and disposal in europe 2006 2010.
Micromeritics autopore iv 9500 series 9505 automated mercury. The latest version of autopore iv 9500 is currently unknown. Oct 18, 2016 autopore iv series mercury porosimeters from micromeritics. The technique offers speed, accuracy, and a wide measurement range.
The pressure required to intrude mercury into the samples pores is inversely proportional to the size of the pores. Pore size distributions, total pore volume, total pore surface area. Benefits includethe calculation of numerous sample properties such as. Clicknotocancelthe analysis,thencontinueeditingthesamplefile. Both mesopore and macropore inter particle voids intrusion. Required background to successfully complete this course, you must. The permeability to gas was determined using a permeameter, as described in the. Clickyestosavethechanges,thenproceedwiththeanalysis. Mercury porosimetry porosity and pore size distribution.
Click the button to the right to learn how to submit sample material for particle size and characterization analyses. A nonwetting contact angle of and nonwetting mercury interfacial tension of 484 mjm2 were assumed to convert the measured intrusion pressures into pore diameters for the different samples. Autopore iv 9500 series measures sample porosity laboratory. The pressure required to intrude mercury into the sample pores is inversely proportional to the size of the pores. Micromeritics autopore iv porosimeters 9500 series. Micromeritics instrument corporation 4356 communications drive norcross, ga 30093 u.
Micromeritics tristar 3020 manual the best free software. Syllabus autopore series basic operator training click here to download full course details instructional goals. Pharmaceuticals porosity and surface area play major roles in the purification, processing, blending, tableting, and. If you have more questions along the way, please contact us. Autopore iv table of contents 9504280101 rev a oct 2015 i table of contents 1. Xpert pro mpd, panalytical x pert pro mpd, icdd pdf2 database 2002, hiscore searchmatch software. Autopore iv series micromeritics pages 1 6 flip pdf download. Micromeritics autopore iv 9500 micromeritics autopore iv 9500 sample report mercury intrusion porosimetry mip is a powerful technique utilized for the evaluation of porosity, pore size distribution, and pore volume among others to characterize a wide variety of solid and powder materials.
Autopore iv 9500 nonwetting fluid mercury intrusion device, by pressure, for pore size distribution determining in solid porous sample. Micromeritics shall not be liable for consequential or other type damages resulting from the use. Autopore series basic operator training learning center. Mercury intrusion porosimetry particle technology labs.
A catalyst characterization laboratory in a single analytical instrument micromeritics autochem ii 2920 chemisorption analyzer is a fully automated instrument capable of conducting a comprehensive array of highly precise chemical adsorption and temperature programmed reaction studies. Autopore iv series micromeritics was published by on. The autopore v series porosimeters from micromeritics use the mercury porosimetry analysis method, in which mercury is introduced into a porous structure under closely monitored pressures. This is called mercury porosimetry, or often, mercury intrusion. Micromeritics autopore v series mercury intrusion porosimeters are available in two models to suit the needs of research and quality assurance laboratories. Micromeritics asap 2020hd surface area analyzer micromeritics autopore iv mercury porosimeter. Micromeritics shall not be liable for consequential or other type damages resulting from the use of any of its products other than the liability stated above. Mercury porosimetry porosity and pore size distribution testing. Mercury porosimetry analysis is based on the ingress of mercury into poresunder strict pressure control. A new generalized equation for estimation of sandstone and. For determining the exact contact angle, micromeritics offers the contact anglometer model 1501. It was initially added to our database on 07082008. Autopore iv series porosimeters pharmaceutical online. Tristar ii 3020 surface area analyzer from micromeritics.
Autopore iv 9500 series specifications general low pressure. Micromeritics offers an evolving product line of porosimeters that deliver fast, reliable, and highresolution porosity data. The autopore iv series is available in four models to best match the needs of individual quality assurance and research labs. You can enter values for the advancing contact angle intrusion. View courses calender autochem ii 2920 basic operator training advanced operator training operator training autopore iv. An mip instrument autopore iv 9500, micromeritics was used to measure the pore size distributions. Mercury intrusion porosimetry up to 60,000 psi for measurement of meso and macro pore size distribution, as well as solid density, particle density, skeletal density. The autopore iv 9605 series has 4 lowpressure ports and 2 highpressure ports for analysis at up to 33,000psia. Physicochemical characterization of chars produced in the.
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